2,6-二甲氧基苯甲酸合成路线 (共 118 条)
反应条件
sulfuric acid 18 h; Reflux;
参考文献
Moghaddam, Firouz Matloubi; Farimani, Mahdi Moridi
Tetrahedron Letters, 2010 , vol. 51, # 3 p. 540 - 542
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene 4 h; Heating;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2188 - 2191
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
参考文献
Novartis AG
Patent: US6653503 B2, 2003 ;
反应条件
hydrogenchloride in dimethyl carbonate (DMC); water
参考文献
Novartis AG
Patent: US6515167 B1, 2003 ;
反应条件
copper quinolate in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
in various solvent(s) T=80°C; 2 h;
参考文献
Yoshino, Tomonori; Imori, Satomi; Togo, Hideo
Tetrahedron, 2006 , vol. 62, # 6 p. 1309 - 1317
反应条件
potassium carbonate in acetone 23 h; Heating;
参考文献
Tsuchida, Eishun; Hasegawa, Etsuo; Komatsu, Teruyuki; Nakata, Taisaku; Nishide, Hiroyuki
Chemistry Letters, 1990 , # 3 p. 389 - 392
反应条件
methanol; diethyl ether
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 121, p. 262
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 124, p. 320
反应条件
Pd(OTf)2; silver carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=100°C;
参考文献
Ouchaou, Kahina; Georgin, Dominique; Taran, Frederic
Synlett, 2010 , # 14 art. no. G18110ST, p. 2083 - 2086
反应条件
thionyl chloride Heating;
参考文献
Horne, Stephen; Rodrigo, Russell
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4520 - 4522