PPh3 in dichloromethane-d2 not isolated, detected by NMR at low temps.;
参考文献
Fortner, Kevin C.; Laitar, David S.; Muldoon, John; Pu, Lihung; Braun-Sand, Sonja B.; Wiest, Olaf; Brown, Seth N.
Journal of the American Chemical Society, 2007 , vol. 129, # 3 p. 588 - 600
→
反应条件
in dichloromethane-d2 Kinetics; at -70 to +20°C; not isolated, detected by NMR;
参考文献
Fortner, Kevin C.; Laitar, David S.; Muldoon, John; Pu, Lihung; Braun-Sand, Sonja B.; Wiest, Olaf; Brown, Seth N.
Journal of the American Chemical Society, 2007 , vol. 129, # 3 p. 588 - 600
sodium dithionite in diethyl ether; water treatment of Et2O soln. of IrO(mes)3 with aq. Na2S2O4 soln.; isolated from ether soln., characterized by NMR;
参考文献
Hay-Motherwell, Robyn S.; Wilkinson, Geoffrey; Hussain-Bates, Bilquis; Hursthouse, Michael B.
Polyhedron, 1993 , vol. 12, p. 2009 - 2012
in diethyl ether soln. of the Grignard reagent added to a soln. of the complex, refluxed (4 h); filtered, evapn. (vac.), brown-black residue extd. (hexane), concd., filtered, concd., filtered, cooled, crystn.; elem. anal.;
参考文献
Hay-Motherwell, Robyn S.; Wilkinson, Geoffrey; Hussain-Bates, Bilquis; Hursthouse, Michael B.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 24 p. 3477 - 3482
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
