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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1467-21-6
合成路线
（共 65 条）
1467-21-6
→
反应条件
64-10-8
苯基脲
反应条件
hydrogen; palladium in acetic acid
参考文献
Liu, Qi; Luedtke, Nathan W.; Tor, Yitzhak
Tetrahedron Letters, 2001 , vol. 42, # 8 p. 1445 - 1447
124-38-9
二氧化碳
+
100-39-0
溴化苄
+
74497-02-2
→
反应条件
1467-21-6
反应条件
1: benzyl bromide With sodium azide in acetonitrile T=95°C; P=1500.15 Torr; 3 h; Inert atmosphereMicrowave irradiation; 2: carbon dioxide; aniline in acetonitrile T=70°C; P=10876.1 Torr; 3 h; Microwave irradiation;
参考文献
Carnaroglio, Diego; Martina, Katia; Palmisano, Giovanni; Penoni, Andrea; Domini, Claudia; Cravotto, Giancarlo
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 2378 - 2386
726-25-0
1-苯甲基-3-苯基-2-硫代脲
→
反应条件
1467-21-6
反应条件
potassium dichloroiodate in water; acetonitrile T=20°C; 0.5 h;
参考文献
Viana, Gil Mendes; De Sequeira Aguiar, Lucia Cruz; De Araujo Ferrao, Jonas; Simas, Alessandro Bolis Costa; Vasconcelos, Marcela Guariento
Tetrahedron Letters, 2013 , vol. 54, # 8 p. 936 - 940
103-50-4
苄醚
+
622-34-4
苯基氰胺
→
反应条件
1467-21-6
反应条件
boron trifluoride diethyl etherate in acetic acid T=40 - 50°C; Ritter Amidation; 2 h; Reagent/catalystSolventTime;
参考文献
Panduranga, Veladi; Basavaprabhu; Sureshbabu, Vommina V.
Tetrahedron Letters, 2013 , vol. 54, # 8 p. 975 - 979
103-71-9
异氰酸苯酯
+
100-46-9
苄胺
→
反应条件
1467-21-6
反应条件
in dichloromethane T=60°C; 5 h; Inert atmosphereSealed reaction vessel;
参考文献
Figlus, Marek; Tarruella, Albert C.; Messer, Anastasia; Sollis, Steven L.; Hartley, Richard C.
Chemical Communications, 2010 , vol. 46, # 24 p. 4405 - 4407
108-86-1
溴代苯
→
反应条件
1467-21-6
反应条件
potassium phosphate; CuI in 1,4-dioxane; N,N-dimethyl-formamide
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
495-18-1
苯甲羟肟酸
+
100-46-9
苄胺
→
反应条件
1467-21-6
反应条件
1: benzoyl hydroxylamine With ethyl 2-cyano-2-(4-nitrophenylsulfonyloxyimino)acetate; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=0°C; Lossen Rearrangement; 1.5 h; 2: benzylamine in tetrahydrofuran T=20°C; Lossen Rearrangement; 4 h; Solvent;
参考文献
Thalluri, Kishore; Manne, Srinivasa Rao; Dev, Dharm; Mandal, Bhubaneswar
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 3765 - 3775
865094-48-0
+
100-46-9
苄胺
→
反应条件
1467-21-6
反应条件
N-methyl-pyrrolidine in toluene T=110°C; 18 h;
参考文献
Gallou, Isabelle; Eriksson, Magnus; Zeng, Xingzhong; Senanayake, Chris; Farina, Vittorio
Journal of Organic Chemistry, 2005 , vol. 70, # 17 p. 6960 - 6963
3422-01-3
N-Boc-苯胺
+
100-46-9
苄胺
→
反应条件
1467-21-6
反应条件
1: phenyl-carbamic acid tert-butyl ester With diiodo monosilane; N-ethyl-N,N-diisopropylamine in dichloromethane T=-30 - -5°C; Elimination; 0.5 h; 2: benzylamine in dichloromethane T=-50 - 20°C; Addition; Further stages.;
参考文献
Gastaldi, Stephane; Weinreb, Steven M.; Stien, Didier
Journal of Organic Chemistry, 2000 , vol. 65, # 10 p. 3239 - 3240
64-10-8
苯基脲
+
100-52-7
苯甲醛
→
反应条件
1467-21-6
反应条件
triethylsilane; trifluoroacetic acid in toluene T=22°C; 18 h;
参考文献
Dube, Daniel; Scholte, Andrew A.
Tetrahedron Letters, 1999 , vol. 40, # 12 p. 2295 - 2298
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