反应条件
1: NEt3 / CHCl3 / 15 h / Ambient temperature
2: 3 M aq. HCl
3: 1.) NaH / 1.) THF, 0.5 h, reflux, 2.) 10 min, reflux
4: 27.6 percent / Bu3SnH, Et3B / toluene; hexane / Heating
View Scheme
参考文献
Ishizaki, Miyuki; Kurihara, Ken-ichi; Tanazawa, Eiko; Hoshino, Osamu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 101 - 110
