反应条件
1: 78.5 percent / ZnI2 / 1,2-dichloro-ethane / 0.5 h / Ambient temperature
2: 97.8 percent / 5percent aq. K2CO3 / methanol / 0.25 h / Heating
3: 68.9 percent / Et3N, 4-(dimethylamino)pyridine (DMAP) / CHCl3 / 26 h / Ambient temperature
4: Bu3SnH, AIBN / benzene / 2 h / Heating
View Scheme
参考文献
Ishizaki, Miyuki; Kurihara, Ken-ichi; Tanazawa, Eiko; Hoshino, Osamu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 101 - 110