4-羟基-9H-氧杂蒽-9-酮合成路线 （共 11 条）
参考文献
Dimroth
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 114
反应条件
chromium(VI) oxide in pyridine; water
12 h; Ambient temperature;
参考文献
Jojima, Teruomi; Takeshiba, Hideo; Kinoto, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 198 - 201
反应条件
1: CuCl; tris[2-(2-methoxyethoxy)ethyl]amine / dioxane / 0.67 h / microwawe irradiation
2: polyphosphoric acid / 24 h / 60 °C
3: 89 percent / AlCl3 / benzene / 1 h / Heating
View Scheme
参考文献
Coelho, Paulo J.; Carvalho, Luis M.; Silva, Jose C.; Oliveira-Campos, Ana M.F.; Samat, Andre; Guglielmetti, Robert
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 117 - 123
反应条件
1: CuCl; tris[2-(2-methoxyethoxy)ethyl]amine / dioxane / 0.67 h / microwawe irradiation
2: polyphosphoric acid / 24 h / 60 °C
3: 89 percent / AlCl3 / benzene / 1 h / Heating
View Scheme
参考文献
Coelho, Paulo J.; Carvalho, Luis M.; Silva, Jose C.; Oliveira-Campos, Ana M.F.; Samat, Andre; Guglielmetti, Robert
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 117 - 123
反应条件
1: 48 percent / pyridinium hydrochloride / 2 h / 190 °C
2: 52 percent / chromic oxide / pyridine; H2O / 12 h / Ambient temperature
View Scheme
参考文献
Jojima, Teruomi; Takeshiba, Hideo; Kinoto, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 198 - 201
反应条件
1: 85 percent / KOH / dimethylsulfoxide / 3 h / 50 °C
2: 30 percent / DEA / 3 h / 210 °C / intramolecular cyclisation of further 3-chloro-6-(2-allyloxyphenoxy)pyridazines
3: 52 percent / chromic oxide / pyridine; H2O / 12 h / Ambient temperature
View Scheme
参考文献
Jojima, Teruomi; Takeshiba, Hideo; Kinoto, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 198 - 201
反应条件
in diphenylether
20 h; Heating;
参考文献
Patolia, Ravji J.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 444 - 447
参考文献
Belter, Randolph K.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 12 p. 1302 - 1307
反应条件
1: sodium ethanolate / 195 - 200 °C
2: sulfuric acid / 48 h / |Reflux
View Scheme
参考文献
Szkaradek, Natalia; Rapacz, Anna; Pytka, Karolina; Filipek, Barbara; Siwek, Agata; Cegla, Marek; Marona, Henryk
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 514 - 522
反应条件
1: sodium ethanolate / 195 - 200 °C
2: sulfuric acid / 48 h / |Reflux
View Scheme
参考文献
Szkaradek, Natalia; Rapacz, Anna; Pytka, Karolina; Filipek, Barbara; Siwek, Agata; Cegla, Marek; Marona, Henryk
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 514 - 522
