反应条件
1.1: copper(l) iodide; potassium carbonate / N,N-dimethyl-formamide / 100 °C / |Inert atmosphere
1.2: 20 h / |Inert atmosphere; |Enzymatic reaction
2.1: N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / 20 °C / |Glovebox; |UV-irradiation
View Scheme
参考文献
O'Sullivan, Steven; Doni, Eswararao; Tuttle, Tell; Murphy, John A.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 474 - 478
Angew. Chem., 2013 , vol. 126, # 2 p. 484 - 488,5
