反应条件
1: 98 percent / SOCl2 / 19 h / 20 °C
2: 0.88 g / 1,3-dicyclohexylcarbodiimide; triethylamine / CH2Cl2 / 18 h / 20 °C
3: NaOH / H2O; dioxane / 21 h / 20 °C
4: 69 percent / 1,3-dicyclohexylcarbodiimide / 1,2-dimethoxy-ethane / 17 h / 20 °C
View Scheme
参考文献
Trotter, Nicholas S.; Brimble, Margaret A.; Harris, Paul W.R.; Callis, David J.; Sieg, Frank
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 501 - 517
