2-羟基-5-甲基苯甲酮合成路线 （共 52 条）
反应条件
sodium lauryl sulfate 7 h; Irradiation;
参考文献
Singh, Anil K.; Sonar, Sanjay M.
Synthetic Communications, 1985 , vol. 15, # 12 p. 1113 - 1122
反应条件
1: benzene With polymer-supported phenyliodine(III) diacetate; sulfuric acid in acetic acid T=20°C; Substitution; 60 h; 2: 2-hydroxy 5-methyl benzaldehyde With sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=60 - 70°C; Substitution; 4.5 h;
参考文献
Chen
Synlett, 2000 , # 8 p. 1175 - 1177
反应条件
boron trifluoride diethyl etherate 0.0333333 h; microwave irradiation;
参考文献
Naeimi, Hossein; Moradi, Leila
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 2 p. 284 - 287
反应条件
1: With dimethyl sulfoxide; trifluoroacetic acid; palladium diacetate T=95°C; 24 h; 2: With water T=70°C; 2 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3551 - 3558
反应条件
AlCl3, aluminium chloride in dichloromethane T=-5 - 25°C;
参考文献
Du, Zhen-Ting; Lu, Jing; Yu, Hong-Rui; Xu, Yan; Li, An-Pai
Journal of Chemical Research, 2010 , # 4 p. 222 - 227
反应条件
sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=50°C; Arylation; 4 h;
参考文献
Xia, Min; Chen, ZhenChu
Synthetic Communications, 2000 , vol. 30, # 3 p. 531 - 536
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 14 h;
参考文献
Mamat, Constantin; Buettner, Stefan; Trabhardt, Tiana; Fischer, Christine; Langer, Peter
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6273 - 6275
反应条件
air; Mn3O4 nanoparticles in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=40°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 31, # 30 p. 4267 - 4270
反应条件
1: 90 percent / P2O5/SiO2 / 24 h / 100 °C 2: 85 percent Spectr. / P2O5/SiO2 / 0.08 h / microwave irradiation View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 1258 - 1270
