2-羟基-5-甲基苯甲酮合成路线 (共 52 条)
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2- T=100 - 110°C;
参考文献
Journal of the Chemical Society, , p. 2816,2818, 2819
Journal of the Chemical Society, , p. 455
反应条件
1: pyridine 2: AlCl3 / 160 °C View Scheme
参考文献
Molecular Pharmacology, , vol. 61, # 3 p. 637 - 648
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux 1.2: 2 h / 0 °C / Reflux 2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux 1.2: 2 h / 0 °C / Reflux 2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
iron(III) chloride on silica T=70 - 72°C;
参考文献
Bendale, Pravin M.; Khadilkar, Bhushan M.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 8 p. 1738 - 1739
反应条件
1: 1) n-BuLi / 1) Et2O, room temperature, 2.5 h 2: TBAF / tetrahydrofuran; hexamethylphosphoric acid triamide / 3 h / 40 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 30 p. 4267 - 4270
参考文献
Sci. Rep. Tohoku Univ., Ser. 1: Phys., Chem., Astron., , vol. # 22, p. 55,58
反应条件
hydrogenchloride T=120°C; Yield given;
参考文献
Bulletin de la Societe Chimique de France, , # 5 p. 848 - 854
反应条件
carbon disulfide; aluminium trichloride Behandeln mit α,α,α-Trichlor-toluol und mit Wasser;
参考文献
Journal of Organic Chemistry, , vol. 19, p. 996,1000
反应条件
1: potassium acetate 2: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge 3: aqueous H2SO4; NaNO2 / anschliessendes Erhitzen View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40