2-羟基-5-甲基苯甲酮合成路线 （共 52 条）
反应条件
1: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge 2: aqueous H2SO4; NaNO2 / anschliessendes Erhitzen View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
1: concentrated aqueous hydrochloric acid 2: potassium acetate 3: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge 4: aqueous H2SO4; NaNO2 / anschliessendes Erhitzen View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
1: concentrated aqueous hydrochloric acid 2: potassium acetate 3: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge 4: aqueous H2SO4; NaNO2 / anschliessendes Erhitzen View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
carbon disulfide; aluminium trichloride Verseifung des entstandenen Aethylaethers durch Erwaermen mit AlCl3 in CS2 auf 60-70grad;
参考文献
Chemische Berichte, , vol. 36, p. 3898
Chemische Berichte, , vol. 31, p. 2694
反应条件
1: 90 percent / P2O5/SiO2 / 24 h / 100 °C 2: 85 percent Spectr. / P2O5/SiO2 / 0.08 h / microwave irradiation View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 1258 - 1270
反应条件
1: 72 percent 2: 1) BuLi, 2) aq. NH4Cl / 1) THF, hexane, -100 deg C, 2) THF, hexane, r.t.; further reagent: tBuLi View Scheme
参考文献
Chemische Berichte, , vol. 116, # 10 p. 3375 - 3405
反应条件
1: Br2, AlCl3 / 10 h / 180 °C 2: 30percent aq. HCl / 120 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , # 5 p. 848 - 854
反应条件
sulfuric acid; sodium nitrite anschliessendes Erhitzen;
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
n-butyllithium; ammonium chloride 1) THF, hexane, -100 deg C, 2) THF, hexane, r.t.; further reagent: tBuLi; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 116, # 10 p. 3375 - 3405
反应条件
sulfuric acid in ethanol 70 h; Irradiation; MechanismProduct distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1893 - 1898
