2-羟基-5-甲基苯甲酮合成路线 (共 52 条)
反应条件
anschliessend Behandeln mit Wasser;
参考文献
Journal of Organic Chemistry, , vol. 19, p. 996,1000
参考文献
Journal of Organic Chemistry, , vol. 19, p. 996,1000
反应条件
potassium hydroxide in methanol
参考文献
Rohm and Haas Company
Patent: US4008319 A1, 1977 ;
反应条件
T=350°C; in der Kalischmelze;
参考文献
Cox
Journal of the American Chemical Society, 1927 , vol. 49, p. 1029
反应条件
potassium hydroxide in ethanol T=78°C; 36 h;
参考文献
Sumathi; Balasubramanian
Tetrahedron Letters, 1990 , vol. 31, # 26 p. 3775 - 3778
参考文献
Mahendra; Doreswamy; Sridhar; Shashidhara Prasad; Khanum; Shashikanth; Venu
Journal of Chemical Crystallography, 2005 , vol. 35, # 6 p. 463 - 467
反应条件
1.1: NaOH / ethanol / 5 h / 20 °C 1.2: 99 percent / dimethylformamide / 12 h / 70 °C 2.1: LDA / tetrahydrofuran / -78 °C 2.2: 60 percent / TiCl3; Li / 1,2-dimethoxy-ethane / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 16 p. 5613 - 5615
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C; Kostanecki acylation; 10 h;
参考文献
Hwang, In-Taek; Lee, Sun-Ah; Hwang, Jin-Soo; Lee, Kee-In
Molecules, 2011 , vol. 16, # 8 p. 6313 - 6321
反应条件
4-(N,N-dimethlyamino)pyridine in toluene Wittig reaction; 72 h; Inert atmosphereReflux;
参考文献
Gallagher, Brian D.; Taft, Benjamin R.; Lipshutz, Bruce H.
Organic Letters, 2009 , vol. 11, # 23 p. 5374 - 5377
反应条件
2: zinc; benzene / Behandeln des Reaktionsprodukts mit Thionylchlorid und Pyridin 3: aqueous hydriodic acid View Scheme
参考文献
Chakravarti; Bera
Journal of the Indian Chemical Society, 1944 , vol. 21, p. 109