4-氨基-1,2,5-恶二唑-3-氯化甲醛肟合成路线 （共 4 条）
反应条件
hydrogenchloride; acetic acid; sodium chloride; sodium nitrite in water T=0 - 15°C; 4 h;
参考文献
THE UNIVERSITY OF CHICAGO; GAJEWSKI, Thomas F.; SPRANGER, Stefani; LEUNG, Michael
Patent: WO2014/66834 A1, 2014 ;
Location in patent: Paragraph 00185 ;
反应条件
potassium carbonate in tetrahydrofuran; water T=10°C; 2.5 h;
参考文献
Lim, Choong Hwan; Kim, Tae Keun; Kim, Kyung Ho; Chung, Kyoo-Hyun; Kim, Jin Seuk
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 5 p. 1400 - 1402
反应条件
potassium carbonate in diethyl ether; water T=10°C; 2.5 h;
参考文献
Lim, Choong Hwan; Kim, Tae Keun; Kim, Kyung Ho; Chung, Kyoo-Hyun; Kim, Jin Seuk
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 5 p. 1400 - 1402
反应条件
potassium carbonate in tetrahydrofuran; water T=10°C; 2.5 h;
参考文献
Kim, Tae Keun; Lee, Byung Woo; Chung, Kyoo-Hyun
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 10 p. 3802 - 3804
