2-氨基-5-溴-6-甲基-4(1H)-喹唑啉酮合成路线 （共 7 条）
反应条件
4-Mercapto-pyridine; potassium hydroxide in ethylene glycol 2 h; Heating;
参考文献
Chen, Wei-Min; Wan, Shan-He
Synthetic Communications, 2007 , vol. 37, # 1 p. 53 - 61
反应条件
triethylamine in tert-butyl methyl ether; N,N-dimethyl-formamide T=4 - 70°C; 13.1667 h; Large scale;
参考文献
Malmgren, Hakan; Baeckstroem, Birthe; Solver, Ellen; Wennerberg, Johan
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1195 - 1200
反应条件
1: 70 percent / peracetic acid; acetic acid; sulfuric acid / 4 h / 60 - 70 °C 2: dimethylformamide / 31 h / Heating View Scheme
参考文献
Chen, Wei-Min; Wan, Shan-He
Synthetic Communications, 2007 , vol. 37, # 1 p. 53 - 61
反应条件
1: 71.4 percent / sulfuric acid / H2O / 0.33 h / Heating 2: 75.3 percent / potassium hydroxide; 4-mercaptopyridine / ethane-1,2-diol / 2 h / Heating View Scheme
参考文献
Chen, Wei-Min; Wan, Shan-He
Synthetic Communications, 2007 , vol. 37, # 1 p. 53 - 61
反应条件
potassium hydroxide in ethylene glycol
参考文献
Chen, Wei-Min; Wan, Shan-He
Synthetic Communications, 2007 , vol. 37, # 1 p. 53 - 61
反应条件
in N,N-dimethyl-formamide 31 h; Heating; Title compound not separated from byproducts;
参考文献
Chen, Wei-Min; Wan, Shan-He
Synthetic Communications, 2007 , vol. 37, # 1 p. 53 - 61
反应条件
potassium hydroxide 2 h; Reflux;
参考文献
Chen, Wei-Min; Cheng, Chao; Li, Bing-Zhou; Ho, Tse-Lok; Cai, Zhao-Shuo; Wang, Yuqiang; Sun, Ping-Hua
Helvetica Chimica Acta, 2008 , vol. 91, # 11 p. 2062 - 2068
