Z-N,N-二甲基-9-十八烯胺合成路线 （共 10 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 6 h; Heating;
参考文献
Nagase; Kuwahara; Tominaga; Sugawara
Agricultural and Biological Chemistry, 1983 , vol. 47, # 1 p. 53 - 58
反应条件
1.1: sodium methylate / methanol; hexane 2.1: sodium methylate / methanol / 2 h / Reflux 2.2: 24.25 h / 0 °C 3.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / Reflux View Scheme
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1.1: sodium methylate / methanol / 2 h / Reflux 1.2: 24.25 h / 0 °C 2.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / Reflux View Scheme
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1: 100 percent / benzene / 1 h / Ambient temperature 2: 36.9 percent / LiAlH4 / diethyl ether / 6 h / Heating View Scheme
参考文献
Nagase; Kuwahara; Tominaga; Sugawara
Agricultural and Biological Chemistry, 1983 , vol. 47, # 1 p. 53 - 58
反应条件
1: LiAlH4 / diethyl ether 2: (i) TsCl, Py, H2O, (ii) LiBr, MeCOEt 3: propan-2-ol View Scheme
参考文献
Epshtein,A.E. et al.
Pharmaceutical Chemistry Journal, 1977 , vol. 11, # 9 p. 1238 - 1242
Khimiko-Farmatsevticheskii Zhurnal, 1977 , vol. 11, # 9 p. 81 - 86
反应条件
1: (i) TsCl, Py, H2O, (ii) LiBr, MeCOEt 2: propan-2-ol View Scheme
参考文献
Epshtein,A.E. et al.
Pharmaceutical Chemistry Journal, 1977 , vol. 11, # 9 p. 1238 - 1242
Khimiko-Farmatsevticheskii Zhurnal, 1977 , vol. 11, # 9 p. 81 - 86
反应条件
lithium aluminium tetrahydride in diethyl ether 0.5 h; Reflux;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
in isopropyl alcohol
参考文献
Epshtein,A.E. et al.
Pharmaceutical Chemistry Journal, 1977 , vol. 11, # 9 p. 1238 - 1242
Khimiko-Farmatsevticheskii Zhurnal, 1977 , vol. 11, # 9 p. 81 - 86
反应条件
in ethanol 28 h; Reflux;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
in ethanol 28 h; Reflux;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
