1-溴-2-(溴二氟甲基)环己烷合成路线 (共 6 条)
反应条件
ethanolamine; copper(l) chloride in tert-butyl alcohol T=80 - 85°C; 24 h;
参考文献
Gonzales, Javier; Foti, Christopher J.; Elsheimer, Seth
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4322 - 4325
反应条件
zinc in diethyl ether 24 h; Ambient temperatureother reaction partner; other solvents, temperature and reaction time; also with addition of CuCl or radical inhibitors - p-dinitrobenzene and hydroquinone; Product distributionMechanism;
参考文献
Wu, Shi-Hui; Liu, Wei-Zhong; Jiang, Xi-Kui
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 854 - 857
反应条件
potassium hydroxide T=150 - 170°C; 5 h;
参考文献
Elsheimer, Seth; Michael, Mariana; Landavazo, Antonio; Slattery, Darlene K.; Weeks, Jennifer
Journal of Organic Chemistry, 1988 , vol. 53, # 26 p. 6151 - 6153
反应条件
potassium hydroxide T=88 - 105°C;
参考文献
Journal of Organic Chemistry, , vol. 53, # 26 p. 6151 - 6153
反应条件
aluminum oxide; potassium fluoride in acetonitrile T=40 - 50°C; 8 h;
参考文献
Hu, Chang-Ming; Chen, Jian
Journal of Fluorine Chemistry, 1994 , vol. 69, # 1 p. 79 - 84
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Hu, Chang-Ming; Chen, Jian
Journal of Fluorine Chemistry, 1994 , vol. 66, # 1 p. 25 - 26
反应条件
potassium hydroxide T=88 - 105°C;
参考文献
Journal of Organic Chemistry, , vol. 53, # 26 p. 6151 - 6153