十甲基-1,9-二氯五硅氧烷合成路线 （共 8 条）
反应条件
water in 1,4-dioxane; diethyl ether; water addn. of H2O (8.3 mol) in dioxane to a soln. of (CH3)2SiCl2 (16.6 mol) in ether;;
参考文献
Patnode, W. I.; Wilcock, D. F.
Journal of the American Chemical Society, 1946 , vol. 68, p. 358 - 363
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Gmelin Handbook: Si: MVol.C, 104, page 286 - 288
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General Electric Co.
Patent: US2381366 , 1945 ;
C. A., 1945 , p. 4890
反应条件
1,4-dioxane; diethyl ether; water
参考文献
Gen.Electric Co.
Patent: US2421653 , 1944 ;
反应条件
aluminium trichloride in neat (no solvent) ((CH3)2SiO)4 and AlCl3 at about 120°C;;
参考文献
Gmelin Handbook: Si: MVol.C, 104, page 286 - 288
反应条件
sodium nitrate T=0°C; 2 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Ivanova, N. P.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 658 - 659
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 699 - 700
反应条件
phosphoric acid T=20°C; various H3PO4 concentration; Rate constantKinetics;
参考文献
Yuzhelevskii, Yu. A.; Sviridova, N. G.; Karpov, G. I.; Markosova, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 6 p. 1342 - 1346,1137 - 1140
反应条件
CuI; triphenylphosphine; (PPh3)2PdCl2 in triethylamine; toluene
参考文献
The Government of the United States of America, as represented by the Secretary of the Navy
Patent: US2011/306744 A1, 2011 ;
反应条件
CuI; triphenylphosphine; (PPh3)2PdCl2 in triethylamine; toluene
参考文献
The Government of the United States of America, as represented by the Secretary of the Navy
Patent: US2011/306744 A1, 2011 ;
参考文献
Andrianov,K.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , p. 2144 - 2146
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 2243 - 2245
