2-二甲基氨基-2-苯基-乙烷酸合成路线 （共 6 条）
反应条件
hydrogenchloride; hydrogen; palladium 10 on activated carbon in methanol P=1810.07 - 2068.65 Torr; 4 h;
参考文献
WO2012/41014 A1, ;
Page/Page column 81 ;
反应条件
sodium tetrahydroborate in 2,2,2-trifluoroethanol 40 h; Reflux;
参考文献
Tajbakhsh, Mahmood; Hosseinzadeh, Rahman; Alinezhad, Heshmatollah; Ghahari, Somayeh; Heydari, Akbar; Khaksar, Samad
Synthesis, 2011 , # 3 art. no. Z26810SS, p. 490 - 496
反应条件
formic acid 4 h; Heating;
参考文献
Shiraiwa, Tadashi; Baba, Yoshihisa; Miyazaki, Hideya; Sakata, Shinji; Kawamura, Seiko; et al.
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 5 p. 1430 - 1437
反应条件
1: 72.1 percent / methanol / 3 h / 20 °C 2: 90.2 percent / aq. formic acid / 4 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 5 p. 1430 - 1437
反应条件
n-butyllithium 1.) THF, -78 deg C, 10 min, 2.) EtOH, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 54, # 42 p. 12923 - 12952
参考文献
Lawson
Journal of the Chemical Society, 1957 , p. 144,149
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King; McMillan
Journal of the American Chemical Society, 1951 , vol. 73, p. 4451
