顺-1,4-二氯-2-丁烯合成路线 (共 65 条)
反应条件
dihydrogen peroxide; magnesium sulfate; methyltrioxorhenium (VII) in tert-butyl alcohol T=25°C; 48 h;
参考文献
Herrmann, Wolfgang A.; Fischer, Richard W.; Marz, Dieter W.
Angewandte Chemie, 1991 , vol. 103, # 12 p. 1706 - 1709
反应条件
(i), (ii) aq. Na2CO3; Multistep reaction;
参考文献
Bahurel,Y. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 2203 - 2208
反应条件
potassium carbonate T=25°C; 96 h; Yield given. Yields of byproduct given;
参考文献
Depres, Jean-Pierre; Greene, Andrew E.
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 928 - 931
反应条件
(i), (ii) aq. Na2CO3; Multistep reaction;
参考文献
Bahurel,Y. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 2203 - 2208
反应条件
Title compound not separated from byproducts;
参考文献
Wilson, Stephen R.; Wiesler, Donald P.
Synthetic Communications, 1980 , vol. 10, # 4 p. 339 - 344
反应条件
potassium carbonate T=25°C; 96 h; Yield given. Yields of byproduct given;
参考文献
Depres, Jean-Pierre; Greene, Andrew E.
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 928 - 931
反应条件
Title compound not separated from byproducts;
参考文献
Wilson, Stephen R.; Wiesler, Donald P.
Synthetic Communications, 1980 , vol. 10, # 4 p. 339 - 344
反应条件
ozone in acetic anhydride T=24°C; Title compound not separated from byproducts;
参考文献
Tempesti, Ezio; Fornaroli, Mirco; Giuffre, Luigi; Montoneri, Enzo; Airoldi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 7 p. 1319 - 1323
反应条件
sodium hydroxide; sulfuric acid in water; isopropyl alcohol; toluene
参考文献
Bayer Aktiengesellschaft
Patent: US5436334 A1, 1995 ;
反应条件
sodium hydride in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Kim, Wan-Joo; Kim, Bong-Jin; Lee, Tae-Suk; Nam, Keun-Soo; Kim, Keun-Jae
Heterocycles, 1995 , vol. 41, # 7 p. 1389 - 1398