2,2,5,5-四甲基-1,3-二氧杂-2-硅杂环己烷合成路线 (共 11 条)
反应条件
sulfuric acid in toluene T=40°C; 8 h;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
sulfuric acid in toluene T=40°C; 8 h; Yield given;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
dimethyl-dichlorosilane in tetrahydrofuran; dichloromethane 0.5 h; Ambient temperature;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Sugiyama, Yoshie; Fukata, Fumio; Haruta, Jun-ichi; Yasumitsu, Tamura
Tetrahedron Letters, 1983 , vol. 24, # 12 p. 1273 - 1276
反应条件
sulfuric acid in toluene T=40°C; 8 h;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
sulfuric acid in toluene T=40°C; 8 h;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
in 1,4-dioxane T=20°C; 0.166667 h;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Lapuka, L. F.; Kantor, E. A.; Sarmanaev, R. S.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 6 p. 670 - 675
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 6 p. 845 - 851
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
参考文献
Voronkov,M.G.; Romadan,Yu.P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1966 , vol. 2, p. 671 - 681
Khimiya Geterotsiklicheskikh Soedinenii, 1966 , vol. 2, # 6 p. 879 - 891
反应条件
in 1,4-dioxane T=20°C;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 61, # 4 p. 937 - 940,856 - 859
反应条件
epoxysulfonyl fluoride T=-70°C; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 56, # 3 p. 617 - 621,545 - 549