2,6-二碘-3-羟基吡啶合成路线 (共 11 条)
反应条件
iodine; potassium carbonate in water 2 h;
参考文献
Bourne, Gregory T.; Kuster, Daniel J.; Marshall, Garland R.
Chemistry - A European Journal, 2010 , vol. 16, # 28 p. 8439 - 8445
反应条件
iodine; sodium carbonate in water T=20°C; 0.5 h; Yields of byproduct given;
参考文献
Koch; Schnatterer
Synthesis, 1990 , # 6 p. 497 - 498
反应条件
iodine; potassium carbonate 1) DMF, 60 deg C; 2) DMF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 3008 - 3009
反应条件
sodium hydroxide; water; iodine
参考文献
Roczniki Chemii, , vol. 27, p. 258,264
Chem.Abstr., , p. 10287
反应条件
water; iodine; sodium carbonate; potassium iodide
参考文献
Roczniki Chemii, , vol. 30, p. 315
Chem.Abstr., , p. 1163
反应条件
water; iodine; sodium carbonate; potassium iodide
参考文献
Chemische Berichte, , vol. 69, p. 2593,2604
参考文献
Roczniki Chemii, , vol. 30, p. 315
Chem.Abstr., , p. 1163
反应条件
1: 2,6-diiodo-3-hydroxypyridine With sodium methylate in N,N-dimethyl-formamide 0.5 h; 2: methyl iodide in N,N-dimethyl-formamide T=20°C; 15 h; Further stages.;
参考文献
Mongin, Florence; Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Queguiner, Guy
The Journal of organic chemistry, 2002 , vol. 67, # 10 p. 3272 - 3276
反应条件
methanol; diethyl ether
参考文献
Burger; Bailey
Journal of the American Chemical Society, 1946 , vol. 68, p. 520
反应条件
sodium hydroxide; water
参考文献
Bojarska-Dahlig; Swirska
Roczniki Chemii, 1953 , vol. 27, p. 258,264
Chem.Abstr., 1955 , p. 10287