二(氰基)二(1,10-菲咯啉)-铁合成路线 (共 5 条)
反应条件
potassium cyanide in water Fe salt aq. soln. heating nearly boiling, aq. KCN adding at once, stirring, cooling to room temp., dark violet crystals collecting, drying in vacuo; identified by IR, UV spectra;
参考文献
Rollick, K. L.; Kochi, J. K.
Organometallics, 1982 , vol. 1, p. 725 - 732
反应条件
potassium cyanide in methanol; water Electrochem. Process; electrochem. oxidn. of Fe wire in MeOH-H2O (2:1) in presence of KCN andC12H8N2 (1:1 mol ratio);
参考文献
Griffiths, Lynne; Straughan, Brian P.; Gardiner, Derek J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 305 - 310
反应条件
sodium chloride; ascorbic acid powder in water Kinetics; Irradiation (UV/VIS); decompn. of aq. soln. of iron complex in the presence of o-phenanthroline (20-45°C, addn. of ascorbic acid, NaCl) under UV-irradiation; UV spect.;
参考文献
Ronco, S. E.; Aymonino, P. J.
Inorganica Chimica Acta, 1987 , vol. 131, p. 113 - 118
反应条件
sodium chloride in water Irradiation (UV/VIS); irradiation of mixt. of aq. complex, o-phenanthroline, NaCl, room temp., >15 min.; products were not isolated; analyzed by UV;
参考文献
Ronco, S. E.; Aymonino, O. J.
Inorganica Chimica Acta, 1983 , vol. 77, p. L31 - L34
反应条件
in water Kinetics; byproducts: 1,10-phenanthroline; in microemulsion, 298 K;
参考文献
Blandamer, Michael J.; Burgess, John; Clark, Barbara
Journal of the Chemical Society, Chemical Communications, 1983 , # 12 p. 659 - 660