2-甲氧基-4-(2-氨基乙基)苯酚合成路线 (共 14 条)
反应条件
potassium carbonate; triethylamine in methanol; chloroform
参考文献
JOH, TONG H.; CHO, SUNGHEE; CHU, CHUNG K.; DU, JINFA
Patent: US2001/11146 A1, 2001 ;
反应条件
1: formic acid With acetic anhydride
T=55°C; 2 h;
2: 2-(4-hydroxy-3-methoxyphenyl)-ethylamine hydrochloride in tetrahydrofuran
T=75°C; 16 h; Further stages.;
参考文献
Lamberth, Clemens; Jeanguenat, Andre; Cederbaum, Fredrik; De Mesmaeker, Alain; Zeller, Martin; Kempf, Hans-Joachim; Zeun, Ronald
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 3 p. 1531 - 1545
参考文献
Jai, Woong Seo; Srisook, Ekaruth; Hyo, Jin Son; Hwang, Onyou; Cha, Young-Nam; Dae, Yoon Chi
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 14 p. 3369 - 3373
反应条件
1: With hydrogenchloride in water
T=100°C; 24 h; Pressure tube;
2: With sodium hydrogencarbonate in water
参考文献
Hwang, On-You; Chi, Dae-Yoon; Son, Hyo-Jin; Seo, Jai-Woong
Patent: US2010/217003 A1, 2010 ;
Location in patent: Page/Page column 4 ;
US 20100217003 A1