3-甲基-2-亚氨基苯并噻唑合成路线 (共 20 条)
反应条件
1: (i), (ii) aq. HClO4, MeOH
2: aq. HClO4 / methanol
View Scheme
参考文献
VanAllan,J.A.; Reynolds,G.A.
Journal of Heterocyclic Chemistry, 1968 , vol. 5, p. 471 - 476
反应条件
bromine in chloroform
参考文献
Barnikow,G.; Boedeker,J.
Chemische Berichte, 1967 , vol. 100, # 5 p. 1394 - 1401
反应条件
1: diethyl ether / -40 °C / Inert atmosphere
2: potassium hydride / 66 °C / Inert atmosphere
View Scheme
参考文献
Coetzee, Jacorien; Cronje, Stephanie; Dobrzanska, Liliana; Raubenheimer, Helgard G.; Joone, Gisela; Nell, Margo J.; Hoppe, Heinrich C.
Dalton Transactions, 2011 , vol. 40, # 7 p. 1471 - 1483
参考文献
Costakis,E. et al.
Canadian Journal of Chemistry, 1969 , vol. 47, p. 4483 - 4488
反应条件
sulfuric acid
Heating;
参考文献
Zhmurova,I.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 1223 - 1227,1193 - 1196
参考文献
Oksengendler
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 135,138; engl. Ausg. S. 133, 136
参考文献
Akiba,K. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 535 - 539
反应条件
1: ethanolic KOH-solution
2: KI
View Scheme
参考文献
Kiprianow; Pasenko
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1521
Chem.Abstr., 1950 , p. 1097
反应条件
in diethyl ether; benzene
T=40 - 60°C;
参考文献
Joshua,C.P.
Journal of the Indian Chemical Society, 1961 , vol. 38, # 12 p. 979 - 987
参考文献
Hunter; Jones
Journal of the Chemical Society, 1930 , p. 2190,2209