in ethanol; water addition of a solution of 0.002 mol salicylaldehyde and 0.002 mol aniline in 10 ml ethanol drop by drop under stirring to a solution of 0.005 mol VOSO4*2H2O in 20 ml water;; recrystallization from toluene;;
参考文献
Ramaiah, K.; Martin, D. F.
Journal of Inorganic and Nuclear Chemistry, 1965 , vol. 27, p. 1663 - 1669
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Gmelin Handbook: V: MVol.B2, 185, page 764 - 766