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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14790-63-7
合成路线
（共 9 条）
100-02-7
对硝基苯酚
→
反应条件
14790-63-7
反应条件
1: sodium hydride; sodium iodide / N,N-dimethyl-formamide 2: thionyl chloride / dichloromethane View Scheme
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
1353638-99-9
→
反应条件
14790-63-7
反应条件
1: hydrazine hydrate / methanol / 4 h / 20 °C 2: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction 3: sodium hydride; sodium iodide / N,N-dimethyl-formamide 4: thionyl chloride / dichloromethane View Scheme
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
1353639-00-5
→
反应条件
14790-63-7
反应条件
1: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction 2: sodium hydride; sodium iodide / N,N-dimethyl-formamide 3: thionyl chloride / dichloromethane View Scheme
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
4527-37-1
→
反应条件
14790-63-7
反应条件
thionyl chloride in dichloromethane
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
100-28-7
异氰酸对硝基苯
→
反应条件
14790-63-7
反应条件
1: triethylamine / toluene / 6 h / 20 °C 2: hydrazine hydrate / methanol / 4 h / 20 °C 3: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction 4: sodium hydride; sodium iodide / N,N-dimethyl-formamide 5: thionyl chloride / dichloromethane View Scheme
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
3459-18-5
4-硝基苯基-2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖苷
→
反应条件
14790-63-7
反应条件
1: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction 2: sodium hydride; sodium iodide / N,N-dimethyl-formamide 3: thionyl chloride / dichloromethane View Scheme
参考文献
Chibba, Anthony; Dasgupta, Somnath; Yakandawala, Nandadeva; Madhyastha, Srinivasa; Nitz, Mark
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 7-9 p. 549 - 558
807291-15-2
→
反应条件
14790-63-7
反应条件
thionyl chloride
参考文献
Barber et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 266,273
Journal of Applied Chemistry, 1954 , vol. 4, p. 110,111
101087-26-7
→
反应条件
14790-63-7
反应条件
1: concentrated aqueous nitric acid 2: thionyl chloride View Scheme
参考文献
Barber et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 266,273
Journal of Applied Chemistry, 1954 , vol. 4, p. 110,111
108-95-2
苯酚
→
反应条件
14790-63-7
反应条件
1: aq. NaOH solution / 220 °C 2: concentrated aqueous nitric acid 3: thionyl chloride View Scheme
参考文献
Barber et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 266,273
Journal of Applied Chemistry, 1954 , vol. 4, p. 110,111
