in benzene
byproducts: (CF3)2C(C6H4)(Cl)(OCOCH2CH2COC2H5); addn. of ethyl succinyl chloride at room temperature; stirring for 8.5 h at 50 ° C;; thin layer chromatography (ethyl acetate:hexane=1:5);;
PhCH2Pd(PPh3)2Cl in acetonitrile-D3
react. of Sb compd. with acid chloride in the presence of Pd-catalyst;
参考文献
Yamamoto, Yohsuke; Okinaka, Takaaki; Nakatani, Masayuki; Akiba, Kin-ya
Nippon Kagaku Kaishi (Journal of the Chemical Society of Japan), 1987 , vol. 62, p. 1286 - 1287