[(3-氯苯基)亚氨基](三苯基)膦烷合成路线 (共 4 条)
反应条件
1: triphenylphosphine With bromine in benzene T=-5 - 20°C; 1.33333 h; Inert atmosphere; 2: 3-chloro-aniline With triethylamine in benzene Inert atmosphereReflux;
参考文献
He, Hua-Feng; Wang, Zhi-Jing; Bao, Weiliang
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2905 - 2912
反应条件
in 1,2-dichloro-ethane T=20°C; Staudinger reaction; 4 h;
参考文献
Yang, Yun-Yun; Shou, Wang-Ge; Hong, Deng; Wang, Yan-Guang
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3574 - 3577
反应条件
1: Br2 / CCl4 2: Et3N / CCl4 / 2 h / Heating View Scheme
参考文献
Braun, Thomas P.; Gutsch, Paul A.; Zimmer, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1999 , vol. 54, # 7 p. 858 - 862
反应条件
triethylamine in tetrachloromethane Condensation; 2 h; Heating;
参考文献
Braun, Thomas P.; Gutsch, Paul A.; Zimmer, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1999 , vol. 54, # 7 p. 858 - 862