[(4-甲氧基苯基)亚氨基](三苯基)膦烷合成路线 (共 11 条)
反应条件
in diethyl ether T=20°C; 2 h;
参考文献
Foster, Robert S.; Adams, Harry; Jakobi, Harald; Harrity, Joseph P. A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4049 - 4064
反应条件
1: triphenylphosphine With bromine in benzene T=-5 - 20°C; 1.33333 h; Inert atmosphere; 2: 4-methoxy-aniline With triethylamine in benzene Inert atmosphereReflux;
参考文献
He, Hua-Feng; Wang, Zhi-Jing; Bao, Weiliang
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2905 - 2912
反应条件
1.1: aq. H2SO4 1.2: NaN3; aq. sodium acetate 2.1: diethyl ether / 2 h / Heating View Scheme
参考文献
Stauffer, Shaun R.; Sun, Jun; Katzenellenbogen, Benita S.; Katzenellenbogen, John A.
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 6 p. 1293 - 1316
参考文献
Horner; Oediger
Justus Liebigs Annalen der Chemie, 1959 , vol. 627, p. 142,147
反应条件
T=25°C; Rate constant;
参考文献
Horner; Gross
Justus Liebigs Annalen der Chemie, 1955 , vol. 591, p. 117,123, 134
参考文献
Alajarin; Molina; Sanchez-Andrada; Foces-Foces
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1121 - 1130
反应条件
in dichloromethane T=20°C; Aza-Wittig reaction; Inert atmosphere;
参考文献
He, Hua-Feng; Wang, Zhi-Jing; Bao, Weiliang
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2905 - 2912
反应条件
1: 83 percent / benzene / 8 h / Heating 2: 71 percent / aqueous Sodium Hydroxide / 1 h / Heating View Scheme
参考文献
Briggs, Elizabeth; Brown, Geoffrey W.; Jiricny, Josef; Meidine, Mohamed F.
Synthesis, 1980 , # 4 p. 295 - 296
反应条件
1: tetrahydrofuran / 3 h / Heating 2: NaBH3CN / tetrahydrofuran / 1 h / 0 - 20 °C View Scheme
参考文献
Hemming; Bevan; Loukou; Patel; Renaudeau
Synlett, 2000 , # 11 p. 1565 - 1568
反应条件
in tetrahydrofuran
Condensation; Aza-Wittig reaction; 3 h; Heating;
参考文献
Hemming; Bevan; Loukou; Patel; Renaudeau
Synlett, 2000 , # 11 p. 1565 - 1568