1: With TentaGel-N(R)C(O)CH2C2F4OC2F4SO2F; potassium carbonate in N,N-dimethyl-formamide T=20°C; 2: With formic acid; 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=85°C; 2 h; Further stages.;
参考文献
Pan, Yijun; Holmes, Christopher P.
Organic Letters, 2001 , vol. 3, # 17 p. 2769 - 2770
in tetrahydrofuran Addn. of Yb-complex soln to soln. of 8-hydroxyquinoline under Ar, stirring 24 h at room temp.; Concg., addn. of n-hexane pptd. a solid, washing (n-hexane), crystn. (THF/n-hexane), elem. anal.;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 19, p. 157 - 168
in tetrahydrofuran Addn. of Nd-complex soln to soln. of 8-hydroxyquinoline under Ar, stirring 24 h at room temp.; Concg., addn. of n-hexane pptd. a solid, washing (n-hexane), crystn. (THF/n-hexane), elem. anal.;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 19, p. 157 - 168
Shreve; Bennett
Journal of the American Chemical Society, 1943 , vol. 65, p. 2243
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Das; Sircar
Journal of the Indian Chemical Society, 1955 , vol. 32, p. 679,681,684
