sulfur dioxide; hydrazine hydrate in ethanol 168 h; Heating;
参考文献
Hegde, Vidyadhar; Hung, Chi-Ying; Madhukar, Puttannachetty; Cunningham, Raymond; Hoepfner, Thomas; Thummel, Randolph P.
Journal of the American Chemical Society, 1993 , vol. 115, # 3 p. 872 - 878
in not given Cu(CH3COO)2*H2O was mixed with ligand, stirred for half an h, to this mixt. 8-hydroxyquinoline was added, stirred for half an h; filtered, washed with H2O, boiled in acetone, dried at 100°C for12 h;
参考文献
Anjaneyulu, Y.; Rao, N. V. S.; Swamy, R. Y.; Rao, R. P.; Pisipati, V. G. K. M.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 2154 - 2158
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Cooling with ice 2.1: 2.5 h / 70 °C / Cooling with ice 3.1: AlCl3, aluminium chloride / anhydrous dichloroethane / 3 h / 80 °C / Cooling with ice 3.2: 20 °C 4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C View Scheme
VARINEL INC; ZURAWSKI JR, Vincent R.; STOUT, David M.; NITZ, Theodore J.
Patent: WO2012/20389 A1, 2012 ;
Location in patent: Page/Page column 22 ;
WO 2012/020389 A1
