N-(氨基磺酰基)氨基甲酸叔丁酯合成路线 （共 7 条）
反应条件
1: in toluene T=0°C; 0.333333 h; 2: With pyridine in toluene T=0°C; 0.666667 h; 3: With ammonium hydroxide in water T=0°C; 2.5 h;
参考文献
Masui, Toshiaki; Kabaki, Mikio; Watanabe, Hideaki; Kobayashi, Tatsuya; Masui, Yoshiyuki
Organic Process Research and Development, 2004 , vol. 8, # 3 p. 408 - 410
反应条件
hydrogen; ammonium formate; palladium on activated charcoal in ethanol T=50°C;
参考文献
Hajri, A.-Houssem; Dewynter, Georges; Criton, Marc; Dilda, Pierre; Montero, Jean-Louis
Heteroatom Chemistry, 2001 , vol. 12, # 1 p. 1 - 5
反应条件
triethanolamine in dichloromethane
参考文献
Vertex Pharmaceuticals Incorporated
Patent: US5723490 A1, 1998 ;
US 5723490 A
反应条件
potassium hydrogencarbonate
参考文献
Vertex Pharmaceuticals Incorporated
Patent: US5723490 A1, 1998 ;
US 5723490 A
反应条件
1: triethylamine / CH2Cl2 / 2 h / 20 °C 2: 86 percent / ammonium formate; H2 / Pd/C / ethanol / 50 °C View Scheme
参考文献
Heteroatom Chemistry, , vol. 12, # 1 p. 1 - 5
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Iso; Irie; Iwaki; Kii; Sendo; Motokawa; Nishitani
Journal of Antibiotics, 1996 , vol. 49, # 5 p. 478 - 484
反应条件
1: triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 4 h / Ambient temperature 2: 69 percent / sodium methoxide / methanol / 0.5 h / -35 °C View Scheme
参考文献
Iso; Irie; Iwaki; Kii; Sendo; Motokawa; Nishitani
Journal of Antibiotics, 1996 , vol. 49, # 5 p. 478 - 484
