1-(1-溴乙基)-4-氯苯合成路线 （共 8 条）
反应条件
potassium hydroxide; dicobalt octacarbonyl; α-methylbenzyl n-butyl ether in butan-1-ol T=35°C; P=760 Torr;
参考文献
Francalanci, F.; Foa, M.
Journal of Organometallic Chemistry, 1982 , vol. 232, # 1 p. 59 - 70
反应条件
in chloroform Kinetics; react. of Sn-compd. with ethane at 90°C for 24 h in a sealed tube; distn.;
参考文献
Kozuka, Seizi; Nakamura, Hisashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2407 - 2410
反应条件
Oxonereg; in water; acetonitrile T=20°C; 1.8 h;
参考文献
Parida, Keshaba Nanda; Jhulki, Samik; Mandal, Susovan; Moorthy, Jarugu Narasimha
Tetrahedron, 2012 , vol. 68, # 47 p. 9763 - 9768,6
Title/Abstract Full Text Show Details
Parida, Keshaba Nanda; Jhulki, Samik; Mandal, Susovan; Moorthy, Jarugu Narasimha
Tetrahedron, 2012 , vol. 68, # 47 p. 9763 - 9768
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 10 p. 1737 - 1740
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere 2.1: potassium hydrogen persulfate / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere 3.2: 0 - 20 °C / Inert atmosphere 4.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Liu, Lei; Henderson, James A.; Yamamoto, Akihiko; Bremond, Paul; Kishi, Yoshito
Organic Letters, 2012 , vol. 14, # 9 p. 2262 - 2265
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 10 p. 1737 - 1740
反应条件
in benzonitrile Kinetics; 110°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 8 p. 2594 - 2598
反应条件
1: NaOEt / ethanol
2: (i) aq. KOH, EtOH, (ii) (decarboxylation)
View Scheme
参考文献
Kuchar; Brunova; Rejholec; et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, # 2 p. 633 - 646
