氯二甲基-3,3,3-氟丙基硅烷合成路线 （共 6 条）
反应条件
RhCl(PPh3)3 T=120°C; 12 h;
参考文献
Ojima, Iwao; Fuchikami, Takamasa; Yatabe, Momoko
Journal of Organometallic Chemistry, 1984 , vol. 260, # 3 p. 335 - 346
反应条件
tri-ruthenium(0)dodecacarbonyl T=120°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 260, # 3 p. 335 - 346
反应条件
in tetrahydrofuran; diethyl ether 18 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 30, # 4 p. 646 - 652
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in toluene T=20°C; ΔG; Equilibrium constantThermodynamic data;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 9 p. 2098 - 2101,1867 - 1870
反应条件
hydrogenchloride; acetic acid; triethylamine in tetrahydrofuran; hexane; water
参考文献
Chisso Corporation
Patent: US5831110 A1, 1998 ;
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in toluene
T=20°C; ΔG; Equilibrium constantThermodynamic data;
参考文献
Nilolaev, G. A.; Mileshkevich, V. P.; Vainshtein, P. M.; Shmeleva, O. A.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 9 p. 2098 - 2101,1867 - 1870
