2-氯-4,4,5,5-四甲基-1,3,2-二氧磷杂环戊烷合成路线 （共 8 条）
反应条件
triethylamine; phosphorus trichoride in diethyl ether T=-10 - 20°C; 2 h;
参考文献
Tromelin, Anne; El Manouni, Driss; Burgada, R.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 301 - 312
反应条件
water in tetrahydrofuran 2 h;
参考文献
Tromelin, Anne; El Manouni, Driss; Burgada, R.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 301 - 312
反应条件
pyridine in chloroform-d1
参考文献
Jiang, Zhi-Hua; Argyropoulos, Dimitris S.; Granata, Alessandro
Magnetic Resonance in Chemistry, 1995 , vol. 33, # 5 p. 375 - 382
反应条件
N,N-dimethyl-aniline in diethyl ether
参考文献
Morita; Kunimoto; Tsuda; Tada; Kise; Kimura
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 10 p. 4144 - 4154
反应条件
1: 66 percent / Et3N / dioxane / 1 h / 20 °C 2: dioxane / 0.1 h / 37 °C View Scheme
参考文献
Bailly, Theodorine; Burgada, Ramon
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 33 - 43
反应条件
in acetonitrile; benzene
8 h; Heating;
参考文献
Ishmaeva, E. A.; Ofitserov, E. N.; Faskhutdinova, T. A.; Zyablikova, T. A.; Ivantaeva, L. P.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 30 - 36,23 - 28
反应条件
pyridine in chloroform-d1
参考文献
Jiang, Zhi-Hua; Argyropoulos, Dimitris S.; Granata, Alessandro
Magnetic Resonance in Chemistry, 1995 , vol. 33, # 5 p. 375 - 382
反应条件
pyridine; diethyl ether; ethanol
参考文献
Arbusow; Asanowskaja
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1949 , p. 473,478
Chem.Abstr., 1950 , p. 1905
