N1,N3-二甲基苯-1,3-二胺合成路线 （共 8 条）
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=0 - 20°C; 2 h; 2: With hydrogenchloride in methanol; water Cooling; 3: With sodium hydroxide in methanol; water
参考文献
Okamoto, Iwao; Terashima, Masayuki; Masu, Hyuma; Nabeta, Mayumi; Ono, Kaori; Morita, Nobuyoshi; Katagiri, Kosuke; Azumaya, Isao; Tamura, Osamu
Tetrahedron, 2011 , vol. 67, # 44 p. 8536 - 8543
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; Reflux;
参考文献
Redko, Boris; Albeck, Amnon; Gellerman, Gary
New Journal of Chemistry, 2012 , vol. 36, # 11 p. 2188 - 2191
反应条件
[((5-Me)PyNPPh2)IrACHTUNGTRENUNG(cod)]; potassium tert-butylate in diethylene glycol dimethyl ether T=70°C; 48 h; Inert atmosphere;
参考文献
Michlik, Stefan; Hille, Toni; Kempe, Rhett
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 847 - 862
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); sodium t-butanolate in tetrahydrofuran; toluene T=85°C; 21 h; Inert atmosphere; chemoselective reaction;
参考文献
Tardiff, Bennett J.; McDonald, Robert; Ferguson, Michael J.; Stradiotto, Mark
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1056 - 1071
反应条件
in diethyl ether T=0 - 25°C; 0.416667 h;
参考文献
Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita
Synthesis, 2003 , # 5 p. 742 - 750
反应条件
1.1: isopentyl nitrite; HCO2H / 0 - 5 °C 2.1: NaOMe / methanol 2.2: 80 percent / methanol / 0.5 h / 20 - 25 °C 3.1: 79 percent / diethyl ether / 0.42 h / 0 - 25 °C View Scheme
参考文献
Redko, Boris; Albeck, Amnon; Gellerman, Gary
New Journal of Chemistry, 2012 , vol. 36, # 11 p. 2188 - 2191
反应条件
und man geloest des Reaktionsprodukts in Methylalkohol,behandelt mit Natriummethylat und Methyljodid und zerlegt das Dimethylformylderivat durch Kochen mit verd.Schwefelsaeure;
参考文献
Fischer,O.
Justus Liebigs Annalen der Chemie, 1895 , vol. 286, p. 173
参考文献
Okamoto, Iwao; Terashima, Masayuki; Masu, Hyuma; Nabeta, Mayumi; Ono, Kaori; Morita, Nobuyoshi; Katagiri, Kosuke; Azumaya, Isao; Tamura, Osamu
Tetrahedron, 2011 , vol. 67, # 44 p. 8536 - 8543
