9,10-二(苯基乙炔基)-9,10-二氢蒽-9,10-二醇合成路线 (共 8 条)
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=-70 - 20°C; 2: 9,10-anthracenedione in tetrahydrofuran; hexane T=-70 - 20°C;
参考文献
Lydon, Donocadh P.; Porres, Laurent; Beeby, Andrew; Marder, Todd B.; Low, Paul J.
New Journal of Chemistry, 2005 , vol. 29, # 7 p. 972 - 976
反应条件
in 1,4-dioxane 15 h; Heating; Further byproducts given;
参考文献
Hanhela, Peter J.; Paul, D. Brenton
Australian Journal of Chemistry, 1981 , vol. 34, p. 1669 - 1686
反应条件
in 1,4-dioxane 15 h; Heating; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hanhela, Peter J.; Paul, D. Brenton
Australian Journal of Chemistry, 1981 , vol. 34, p. 1669 - 1686
反应条件
(i) LiNH2, dioxane, (ii) /BRN= 3102486/; Multistep reaction;
参考文献
Ried,W. et al.
Chemische Berichte, 1961 , vol. 94, p. 1051 - 1058
反应条件
hydrogen iodide in diethyl ether; water
参考文献
Hanhela, Peter J.; Paul, D. Brenton
Australian Journal of Chemistry, 1981 , vol. 34, p. 1669 - 1686
反应条件
tin(ll) chloride in acetic acid Further byproducts given;
参考文献
Australian Journal of Chemistry, , vol. 34, p. 1669 - 1686
反应条件
sodium hypophosphite; potassium iodide in acetic acid 0.5 h; Heating;
参考文献
Australian Journal of Chemistry, , vol. 34, p. 1669 - 1686
反应条件
formic acid 4 h; Heating;
参考文献
Australian Journal of Chemistry, , vol. 34, p. 1669 - 1686