(2S)-(+)-1,1-二(4-甲氧苯基)-3-甲基-1,2-丁二胺合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr; 24 h; Ambient temperature;
参考文献
Wey, Shiow-Jyi; O'Connor, Kenneth J.; Burrows, Cynthia J.
Tetrahedron Letters, 1993 , vol. 34, # 12 p. 1905 - 1908
反应条件
1: 64 percent / tetrahydrofuran / 24 h / Ambient temperature 2: 74 percent / pyridine / CHCl3 / 1 h / 0 °C 3: 95 percent / NaN3, TFA / CHCl3 / a) 0 deg C, 1 h, b) r.t., 4 h 4: 85 percent / H2 / 10 percent Pd/C / ethanol / 24 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 12 p. 1905 - 1908
反应条件
1: 74 percent / pyridine / CHCl3 / 1 h / 0 °C 2: 95 percent / NaN3, TFA / CHCl3 / a) 0 deg C, 1 h, b) r.t., 4 h 3: 85 percent / H2 / 10 percent Pd/C / ethanol / 24 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 12 p. 1905 - 1908
反应条件
1: 95 percent / NaN3, TFA / CHCl3 / a) 0 deg C, 1 h, b) r.t., 4 h 2: 85 percent / H2 / 10 percent Pd/C / ethanol / 24 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 12 p. 1905 - 1908
反应条件
1: 64 percent / tetrahydrofuran / 24 h / Ambient temperature 2: 74 percent / pyridine / CHCl3 / 1 h / 0 °C 3: 95 percent / NaN3, TFA / CHCl3 / a) 0 deg C, 1 h, b) r.t., 4 h 4: 85 percent / H2 / 10 percent Pd/C / ethanol / 24 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 12 p. 1905 - 1908
