2,4,6-三苯基吡喃鎓高氯酸盐合成路线 (共 65 条)
反应条件
perchloric acid; trichlorophosphate
1.) room temp., 14 h; 50 deg C, 3 h; 2.) EtOH; Yield given. Multistep reaction;
参考文献
Schroth, Werner; Spitzner, Roland; Freitag, Joerg
Synthesis, 1983 , # 10 p. 827 - 830
反应条件
in methanol
T=25°C; Equilibrium constantRate constant;
参考文献
Doddi, Giancarlo; Ercolani, Gianfranco; Nunziante, Patrizia
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1427 - 1430
反应条件
in methanol
T=25°C; Equilibrium constantRate constant;
参考文献
Doddi, Giancarlo; Ercolani, Gianfranco; Nunziante, Patrizia
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1427 - 1430
反应条件
in neat (no solvent)
T=0°C; 7 h;
参考文献
Harris, D. J.; Kan, G. Y.-P.; Tschamber, T.; Snieckus, V.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 494 - 500
反应条件
1: piperidine acetate / acetonitrile / 20 h / Heating
2: 10 percent NaOH / ethanol; H2O / 0.5 h / Heating
View Scheme
参考文献
Zimmermann, Thomas; Fischer, Gerhard W.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 3 p. 499 - 510
反应条件
in N,N-dimethyl-formamide
Heating;
参考文献
Zvezdina, E. A.; Zhdanova, M. P.; Anisimova, O. S.; Dorofeenko, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 564 - 571
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 695 - 701
反应条件
tert-butyl alcohol
1 h; Heating; Yield given;
参考文献
Zimmermann, Thomas; Fischer, Gerhard W.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 775 - 788
反应条件
sodium tetrahydroborate; acetic acid
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Balaban, Teodor-Silviu; Balaban, Alexandru, T.
Tetrahedron Letters, 1987 , vol. 28, # 12 p. 1341 - 1344
参考文献
Zvezdina, E. A.; Zhdanova, M. P.; Anisimova, O. S.; Dorofeenko, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 564 - 571
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 695 - 701
反应条件
triethylamine in acetic anhydride
Condensation; substitution; 30 h; Heating;
参考文献
Oganesyan; Pyshchev; Butenko
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 9 p. 480 - 483