1-[(2-羟基-5-硝基苯基)偶氮]-2-萘酚合成路线 (共 2 条)
反应条件
1: 2-amino-4-nitro-phenol With hydrogenchloride; sodium nitrite in water
T=0 - 5°C;
2: β-naphthol With sodium hydroxide in methanol; water
T=5°C;
参考文献
Satam, Manjaree A.; Sekar, N.; Raut, Rajesh K.
Dyes and Pigments, 2013 , vol. 96, # 1 p. 92 - 103,12
反应条件
sodium hydroxide; sulfuric acid; nitric acid; acetic acid; sodium nitrite
1.) 70-80 deg C, 2 h, 2.) H2O, 20 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gorelik; Shteiman; Shner; Romanskii; Kuznetsova
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 3 p. 348 - 352