2,6-二氯-3-吡啶硼酸合成路线 （共 3 条）
反应条件
1: With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-80°C; 1 h; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-80 - 20°C;
参考文献
Voisin, Anne Sophie; Bouillon, Alexandre; Lancelot, Jean-Charles; Rault, Sylvain
Tetrahedron, 2005 , vol. 61, # 6 p. 1417 - 1421
反应条件
dihydrogen peroxide in dichloromethane; water T=20°C; 20 h;
参考文献
Voisin, Anne Sophie; Bouillon, Alexandre; Lancelot, Jean-Charles; Rault, Sylvain
Tetrahedron, 2005 , vol. 61, # 6 p. 1417 - 1421
反应条件
1: dihydrogen peroxide / dichloromethane; water / 0.15 h / 0 - 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C View Scheme
参考文献
MERCK SHARP and DOHME CORP.; MCCOMAS, Casey Cameron; LIVERTON, Nigel J.; HABERMANN, Joerg; KOCH, Uwe; NARJES, Frank; LI, Peng; PENG, Xuanjia; SOLL, Richard; WU, Hao; PALANI, Anandan; HE, Shuwen; DAI, Xing; LIU, Hong; LAI, Zhong; LONDON, Clare; XIAO, Dong; ZORN, Nicolas; NARGUND, Ravi
Patent: WO2013/33971 A1, 2013 ;
