四(三氟甲基)二磷杂硫杂环己烷合成路线 (共 32 条)
反应条件
between -196°C and -50°C within 7 h;
参考文献
Gosling,K.; Burg,A.B.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2011 - 2015
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Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
参考文献
Gosling,K.; Burg,A.B.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2011 - 2015
反应条件
Hg
20°C (3 d); shaking with Hg in excess;
参考文献
Dobbie,R.C. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2015 - 2020
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Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
反应条件
triethyl amine
slow warming from -196°C to -40 - -35°C;
参考文献
Burg, A. B.; Gosling, K.
Journal of the American Chemical Society, 1965 , vol. 87, p. 2113 - 2116
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Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
参考文献
Burg, A. B.; Gosling, K.
Journal of the American Chemical Society, 1965 , vol. 87, p. 2113 - 2116
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Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
反应条件
mercury
20°C (4 d); shaking;
参考文献
Pinkerton,A.A.; Cavell,R.G.
Journal of the American Chemical Society, 1971 , vol. 93, p. 2384 - 2390
参考文献
Pinkerton,A.A.; Cavell,R.G.
Journal of the American Chemical Society, 1972 , vol. 94, p. 1870 - 1874
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Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
反应条件
H2S
hardly separable mixture;
参考文献
Gosling,K.; Burg,A.B.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2011 - 2015
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
参考文献
Dobbie,R.C. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2015 - 2020
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
反应条件
100°C (7 d); 21percent (CF3)2PSP(CF3)2;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.9, page 70 - 123