反应条件
in diethyl ether byproducts: CH4; (N2), dried solvents, -40°C, dropwise addn. of educts, 4 h, evapn. in vac. (same temp.), addn. of petroleum ether yield yellow pptn., cooled down to -78°C; filtration ppt., washing (pentane), dried (high vac.), elem. anal.;
参考文献
Schubert, Ulrich; Mueller, Christine
Journal of Organometallic Chemistry, 1989 , vol. 373, p. 165 - 172
