1: 3-azido-2-cyclohexen-1-one; methyl(diphenyl)-phosphine in dichloromethane T=20°C; Substitution; Staudinger reaction; 0.5 h; 2: 4-nitrobenzaldehdye in chloroform T=45°C; Addition; aza-Wittig reaction; Title compound not separated from byproducts;
参考文献
Palacios, Francisco; Herran, Esther; Rubiales, Gloria
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6239 - 6246
Fukuzumi, Shunichi; Shimoosako, Kanji; Suenobu, Tomoyoshi; Watanabe, Yoshihito
Journal of the American Chemical Society, 2003 , vol. 125, # 30 p. 9074 - 9082
in various solvent(s) T=135°C; other atomtransfer (S and Se) reactions; Rate constantEquilibrium constant;
参考文献
Baechler, Raymond D.; Stack, Mary; Stevenson, Karen; Vanvalkenburgh, Virginia
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 49 - 52
