4-苯甲氧基苯(甲)酰氯合成路线 （共 47 条）
参考文献
Wako Pure Chemical Industries, Ltd.; Nippon Telegraph and Telephone Corporation
Patent: US5114615 A1, 1992 ;
反应条件
1: methanolic KOH-solution 2: benzene; phosphorus pentachloride View Scheme
参考文献
Journal of the Chemical Society, , vol. 97, p. 1747
反应条件
1: sodium methylate 2: methanolic KOH-solution 3: benzene; phosphorus pentachloride View Scheme
参考文献
Journal of the Chemical Society, , vol. 97, p. 1747
反应条件
1: 88 percent / potassium permanganate, magnesium sulfate / acetone / 0.5 h / Ambient temperature 2: 98 percent / oxalyl chloride, DMF / CH2Cl2 / 2 h View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 72, # 10 p. 2137 - 2143
反应条件
tri-n-butyl-tin hydride in 1-methyl-pyrrolidin-2-one T=20°C; Inert atmosphere;
参考文献
Le Menez, Patrick; Hamze, Abdallah; Provot, Olivier; Brion, Jean-Daniel; Alami, Mouad
Synlett, 2010 , # 7 p. 1101 - 1103
反应条件
in pyridine T=50 - 80°C; 2 h;
参考文献
Horie, Tokunaru; Kawamura, Yasuhiko; Yamamoto, Hitoshi; Kitou, Takeshi; Yamashita, Kazuyo
Phytochemistry (Elsevier), 1995 , vol. 39, # 5 p. 1201 - 1210
反应条件
pyridine anschliessend Behandeln mit wss. HCl und Eis;
参考文献
Flores et al.
Tetrahedron, 1958 , vol. 4, p. 132
反应条件
1: NEt3, 4-pyrrolidinopyridine / CH2Cl2 / 3 h / Heating 2: H2 / 10percent Pd-C / CH2Cl2; tetrahydrofuran / 3375.3 Torr View Scheme
参考文献
Deschenaux, Robert; Marendaz, Jean-Luc; Santiago, Julio
Helvetica Chimica Acta, 1993 , vol. 76, # 2 p. 865 - 876
反应条件
1: pyridine / 24 h 2: 1) NaOH, 2) H2O / 1) ether, DMSO, 15 min, 2) 45 min 3: 61 percent / H2 / Pd-C / ethanol 4: 0.03 h / 200 °C View Scheme
参考文献
Hauteville, Marcelle; Chopin, Jean; Geiger, Hans; Schuler, Lothar
Tetrahedron, 1981 , vol. 37, p. 377 - 381
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice; Inert atmosphere 2: potassium tert-butylate / tetrahydrofuran / 1 h / Reflux; Inert atmosphere 3: toluene-4-sulfonic acid / benzene / 7 h / Reflux; Inert atmosphere 4: 20 palladium hydroxide on charcoal; hydrogen / ethanol; ethyl acetate / 2 h / 20 °C / Inert atmosphere 5: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 23 p. 7085 - 7092
