3,4-二(苄氧基)苯甲酰氯合成路线 （共 14 条）
反应条件
1: 2.2 g / pyridine / 1 h / Heating
2: 1.8 g / KOH, pyridine / pyridine / 3 h
3: 1.5 g / fused sodium acetate, glacial acetic acid / 4 h / Heating
4: H2 / 10percent Pd/C
5: 0.15 g / AlCl3 / acetonitrile / 2 h / Heating
View Scheme
参考文献
Bhardwaj, D. K.; Gupta, A. K.; Jain, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 9 p. 800 - 801
反应条件
1: 2.2 g / pyridine / 1 h / Heating
2: 1.8 g / KOH, pyridine / pyridine / 3 h
3: 1.5 g / fused sodium acetate, glacial acetic acid / 4 h / Heating
4: H2 / 10percent Pd/C
View Scheme
参考文献
Bhardwaj, D. K.; Gupta, A. K.; Jain, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 9 p. 800 - 801
反应条件
in dichloromethane
T=0°C; 2 h;
参考文献
Greenhouse, Robert; Ramirez, Coral; Muchowski, Joseph M.
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2961 - 2965
反应条件
1: pyridine / 3 h / 120 °C
2: KOH, pyridine / 4 h / 60 °C
3: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C
4: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate
View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
