2,4-二氯-4’-氨基二苯醚合成路线 （共 8 条）
反应条件
hydrazine hydrate; nickel in ethanol; 1,2-dichloro-ethane T=50 - 60°C; 4 h;
参考文献
Ayyangar, N. R.; Lugade, A. G.; Nikrad, P. V.; Sharma, V. K.
Synthesis, 1981 , # 8 p. 640 - 643
反应条件
hydrogenchloride in diethyl ether; water; isopropyl alcohol
参考文献
ZENECA LIMITED
Patent: EP355049 A3, 1990 ;
反应条件
1: water / Eindampfen des Reaktionsgemisches und Erhitzen des Rueckstands auf 150-170grad View Scheme
参考文献
Journal of the American Chemical Society, , vol. 52, p. 1205,1207
反应条件
sulfuric acid in ethanol T=20°C; MechanismRate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1377 - 1382
反应条件
1: (i) aq. HCl, AcOH, (ii) NaNO2, aq. HBF4 2: (i) Ac2O, (ii) aq. NaOH, MeOH View Scheme
参考文献
Hoechst
Patent: DE2136828 , 1973 ;
Chem.Abstr., 1973 , vol. 78, # 124297
参考文献
Raiford; Thiessen; Wernert
Journal of the American Chemical Society, 1930 , vol. 52, p. 1205,1207
反应条件
triethylamine in chloroform
T=50°C; 2 h;
参考文献
Young, Soo Keum; Young, Ju Lee; Kim, Jeong-Han
Journal of Agricultural and Food Chemistry, 2008 , vol. 56, # 19 p. 9146 - 9151
参考文献
Miyauchi; Endoh; Uematsu
Bulletin of Environmental Contamination and Toxicology, 1995 , vol. 55, # 3 p. 446 - 452
