1-棕榈酰-3-O-苄基-外消旋-甘油合成路线 （共 8 条）
反应条件
pyridine in chloroform T=20°C; Acylation; 48 h;
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
反应条件
silver(l) oxide in dichloromethane T=20°C; 5 h;
参考文献
Tetrahedron, , vol. 59, # 16 p. 2921 - 2928
反应条件
1: 98 percent / hydrogen / Pd/C / ethyl acetate / 72 h / 20 °C 2: 33 percent / silver(I) oxide / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 59, # 16 p. 2921 - 2928
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane T=0°C;
参考文献
Tetrahedron Letters, , vol. 29, # 30 p. 3631 - 3634
反应条件
1.1: NaNH2 / benzene / 1 h / Heating 1.2: 57 percent / benzene / 24 h / Heating 2.1: AcOH / propan-2-ol; H2O / 6 h / Heating 3.1: 30 percent / Py / CHCl3 / 48 h / 20 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 43, # 9 p. 943 - 969
反应条件
1: AcOH / propan-2-ol; H2O / 6 h / Heating 2: 30 percent / Py / CHCl3 / 48 h / 20 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 43, # 9 p. 943 - 969
反应条件
1: Py 2: Br2 3: H2 / Pd 4: Zn / acetone View Scheme
参考文献
Volkova,L.V. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 3 p. 550 - 554,547 - 550
反应条件
triethylamine in benzene
Acylation; 1 h; Heating;
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
