(2,2-联吡啶)二氯钯(II)合成路线 （共 41 条）
反应条件
nitrogen in tetrahydrofuran byproducts: CuCl, aniline; Pd-compd. in THF and CuCl2(PhNH2)2 in a Cu/Pd molar ratio of 4:1 are loaded sep. in the 2 branches of an inverted-Y glass reactor. Reactor is closed under N2, contents are mixed and stirred.; Identification of carbamate obtained by IR and MS spectra.;
参考文献
Journal of Organometallic Chemistry, , vol. 470, # 1.2 p. 249 - 252
反应条件
[2,2']bipyridinyl in tetrahydrofuran the suspn. of the Pd-compd. in THF is stirred with CuCl2 in THF in a closed glass reactor under N2 for 1 h, filtn. (in the liquid phase is CH3OCOCl, detected by IR), addn. of bipy in MeOH to the residue; filtn. (the residue is the Pd-compd., elem. anal.), soln. is evapd. in vac., elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 451, # 1.2 p. 243 - 248
反应条件
1: 1,2-dichloro-ethane 2: dichloromethane View Scheme
参考文献
Organometallics, , vol. 20, # 6 p. 1109 - 1114
反应条件
in dichloromethane byproducts: C6H(OMe)3-4m5m6-(CHO)-2-(SC6H4Me-4)-1; a mixt. in CH2Cl2 was stirred for 1 h; filtered,;
参考文献
Organometallics, , vol. 20, # 6 p. 1109 - 1114
反应条件
in ethanol on react. with α,α-dipyridine in alc. soln., forming of intermediate, decompn. of intermediate;;
参考文献
Journal of the Chemical Society, , p. 2089 - 2089
反应条件
in benzene react. PdCl(CON(CH2)4O)(dipy) with stream Cl2 in benzene at room temp.;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in benzene react. PdCl(CON(CH2)5)(dipy) with stream Cl2 in benzene at room temp.;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in benzene react. Pd(CON(CH2)4O)2(dipy) with stream Cl2 in benzene at room temp.;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in benzene react. Pd(CON(CH2)5)2(dipy) with stream Cl2 in benzene at room temp.;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
反应条件
in tetrahydrofuran react. PdCl(CONC3H7)(dipy) with N-chlorosuccinimide;
参考文献
Organometallics, , vol. 19, # 19 p. 3879 - 3889
