双(氰苯)二氯铂(II)合成路线 （共 24 条）
反应条件
in dichloromethane reduction of solvent in vac. led to the pptn. of a mixture of cis and trans isomers, identified by their soln. 31P NMR spectra;
参考文献
Journal of the American Chemical Society, , vol. 104, # 2 p. 438 - 445
反应条件
in dichloromethane for 1 h at room temp.;
参考文献
Organometallics, , vol. 24, # 11 p. 2764 - 2772
反应条件
in benzene according to R. Bender, P. Braunstein, A. Tiripicchio and C. M. Tiripicchio, J. Chem. Soc., Chem. Commun., 42 (1984); CO atm.; mixture stirred (4 h); homogenization step; after 15 min yellow ppt.;; washing (benzene/hexane); dried in vac.;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 2360 - 2362,2188 - 2190
反应条件
in dichloromethane reduction of solvent in vac. led to the pptn. of a mixture of cis and trans isomers, identified by their soln. 31P NMR spectra;
参考文献
Journal of the American Chemical Society, , vol. 104, # 2 p. 438 - 445
反应条件
in dichloromethane for 1 h at room temp.;
参考文献
Organometallics, , vol. 24, # 11 p. 2764 - 2772
反应条件
in benzene according to R. Bender, P. Braunstein, A. Tiripicchio and C. M. Tiripicchio, J. Chem. Soc., Chem. Commun., 42 (1984); CO atm.; mixture stirred (4 h); homogenization step; after 15 min yellow ppt.;; washing (benzene/hexane); dried in vac.;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 2360 - 2362,2188 - 2190
反应条件
in dichloromethane stirring (10 min); pptn. with pentane, filtration, washing (pentane), drying (vac.);
参考文献
Albinati; Affolter; Pregosin
Organometallics, 1990 , vol. 9, # 2 p. 379 - 387
反应条件
in chloroform equilibrium reaction, at 25°C; detected by (13)C NMR;
参考文献
Rochon, Fernande D.
Canadian Journal of Chemistry, 1996 , vol. 74, # 2 p. 144 - 152
反应条件
in dichloromethane reduction of solvent in vac. led to the pptn. of a mixture of cis and trans isomers, identified by their soln. 31P NMR spectra;
参考文献
Journal of the American Chemical Society, , vol. 104, # 2 p. 438 - 445
反应条件
in dichloromethane for 1 h at room temp.;
参考文献
Organometallics, , vol. 24, # 11 p. 2764 - 2772
